KING FAHD UNIVERSITY OF PETROLEUM & MINERALS

  CHEM 202 LABORATORY SYLLABUS (062)

TEXT: WILLIAMSON,   ORGANIC EXPERIMENTS, 9th edition

 

Dr. Ian Forristal

ROOM #4/116

Tel: 3065

E-mail: ianf@kfupm.edu.sa

Dr. Hasan A. Al-Muallem

ROOM# 4/233

Tel: 2378

E-mail: hmuallem@kfupm.edu.sa

Dr. Jimoh Tijani

ROOM# 4/110

Tel: 2605

E-mail: jtijani@kfupm.edu.sa

 

WK

BEGIN

READING ASSIGNMENT

Analysis

PROBLEMS

1

17-Feb

NO LABORATORY

 

 

2

24-Feb

Electrophilic Aromatic Substitution:
Nitration of Methyl Benzoate

CHAPTER #28, PAGE 309- 313 (310-312).

m.p.
same day

#1,2,4

3

3-March

The Sandmeyer Reaction: 2-Iodobenzoic Acid,
CHAPTER #45, Expt. 4, Page 444-450 (449-450)

m.p.
same day

#1

4

10-March

IR and NMR Spectroscopy,
CHAPTER #12, p. (155-176), and
CHAPTER #13, p. (177-195).

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#1,2,3,4

5

17-March

Reactions of Carbonyl Compounds,
Classification Tests.

CHAPTER #36, EXPT. 2, 4, 5 & 6, Page 364-382 (371-375)

m.p.
same day

#1,2,3,4,5,6,7,8,9,10

6

24-March

The Thiamine Catalyzed Benzoin Condensation,
CHAPTER #54, EXPT. 2, PAGE 521-525 (524)

 

m.p.
next week

#1,2,3,4

7

31-March

Part #A: Benzil from Benzoin,
CHAPTER #55, EXPT. 1, PAGE 526-531 (528).

Part #B: Borohydride Reduction of Benzil,
CHAPTER #56, PAGE 532-534 (532-533).

I.R.

 

I.R.

#1,2

 

#1

8

7-April

Diels-Alder Reaction: cis-Norbornene-5,6-endo-dicarboxylic acid,
CHAPTER #49, EXPT. 2 & 3, PAGE 489-501 (493-495).

1H NMR
next day

#1,2

9

14-April

**********NO LABS************Midterm Vacation********

 

 

10

21-April

Grignard Reactions: Triphenylmethanol,
CHAPTER #38, EXPT. 1, 2 & 4, PAGE 388-400 (392-397)

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#1,2,3,4

11

28-April

Grignard Reaction: Triphenylmethanol continued,

CHAPTER # 38, EXPT. 4, PAGE 388-400 (396-397)

m.p.
same day

 

12

5-May

Dibenzalacetone by the Aldol Condensation,
CHAPTER #37, EXPT. 1, PAGE 383- 387 (384).

m.p.
same day

#1,2,3,4,5,6

13

12-May

Acetanilide from Nitrobenzene,
CHAPTER #46, EXPT. 1 & 2, PAGE 451-463 (456-457)

 

m.p.
next week

 

14

19-May

Sulfanilamide from Acetanilide,

CHAPTER #46, EXPT. 3, PAGE 451-463 (458-460)

 

m.p.
next week

#1,2,3,4

15

26-May

Amines: Solubility and Hinsberg Test,
CHAPTER #43, EXPT. 1 & 2, PAGE 429-438 (431-433).

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#1,2,6